Synthesis and Characterization of Magnetic Iron Oxide Nanoparticles by Co-Precipitation Method at Different Conditions

  • Ahmed Faiq Al-Alawy College of Engineering-University of Baghdad
  • Entisar Eliwi Al-Abodi College of Education Ibn Al-Haitham-University of Baghdad
  • Raya Mohammed Kadhim Ministry of health and environment-Department of International Environment Relationships
Keywords: magnetic nanoparticles, iron oxide, co-precipitation.

Abstract

Magnetic nanoparticles (MNPs) of iron oxide (Fe3O4) represent the most promising materials in many applications. MNPs have been synthesized by co-precipitation of ferric and ferrous ions in alkaline solution. Two methods of synthesis were conducted with different parameters, such as temperature (25 and 80 ̊C), adding a base to the reactants and the opposite process, and using nitrogen as an inert gas. The product of the first method (MNPs-1) and the second method (MNPs-2) were characterized by x-ray diffractometer (XRD), Zeta Potential, atomic force microscope (AFM) and scanning electron microscope (SEM). AFM results showed convergent particle size of (MNPs-1) and (MNPs-2) with (86.01) and (74.14) nm respectively. Also, the zeta potential values of (MNPs-1) and (MNPs-2) were (2.77) and (-12.48) mV, respectively, which indicates more stability of (MNP-2).

 

Published
2018-10-01