Review of Lab-Accelerated Aging Techniques of Asphalt Mixes

Main Article Content

Haydar Raheem Hmoud
Nabeel N. Salman
Mansura Dmytro

Abstract

Bitumen aging contributes to main pavement distress due to the changes in rheological, chemical, and physical characteristics of bitumen. Mainly, aging process can be divided into two categories, the first category namely short-term aging takes place during the heating up of bitumen and aggregate, mixing, transportation, laying down, and compaction. While the second category of aging takes place during the service life of pavement which is denoted as long-term aging. Consequently, researchers’ focus is to simulate bitumen aging in the lab by developing lab-accelerated methods to simulate the process of bitumen aging and studying the rate of change before and after aging. This article reviews these methods and compares the extent of the impact on lab-aged bitumen with old bitumen. The main outcome is, that the duration of exposure to high temperatures, which is the dominant method to accelerate aging process, resulted in inadequate changes in the structure of the bitumen molecule, hence, making it different from old bitumen. For that reason, using oxidants such as hydrogen peroxide showed more reliable results but requires more attention by researchers to achieve a standardized aging process of bitumen.

Article Details

How to Cite
“Review of Lab-Accelerated Aging Techniques of Asphalt Mixes” (2024) Journal of Engineering, 30(06), pp. 1–18. doi:10.31026/j.eng.2024.06.01.
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Articles

How to Cite

“Review of Lab-Accelerated Aging Techniques of Asphalt Mixes” (2024) Journal of Engineering, 30(06), pp. 1–18. doi:10.31026/j.eng.2024.06.01.

Publication Dates

Received

2023-10-16

Accepted

2024-05-31

Published Online First

2024-06-01

References

AASHTO (T 315-12), 2010. Standard method of test for determining the rheological properties of asphalt binder using a dynamic shear rheometer (DSR). The American Association of State Highway and Transportation Officials.

Abbas, D.F. and Al Mosawe, H., 2021. The use of sbs-modified binder to eliminate the aggregate gradation deviation effects in asphalt mixtures. Journal of Engineering, 27(10), pp.68-85. Doi:10.31026/j.eng.2021.10.05

Abutalib, N., Fini, E.H., Aflaki, S. and Abu-Lebdeh, T.M., 2015. Investigating effects of application of silica fume to reduce asphalt oxidative aging. American Journal of Engineering and Applied Sciences, 8(1), pp.176-184. Doi:10.3844/ajeassp.2015.176.184

Airey, D. and Prathapa, R., 2013. Triaxial testing of asphalt. In Proceedings of 18th International Conference on Soil Mechanics and Geotechnical Engineering, Paris, pp. 301-304.

Airey, G.D., 1997. Rheological characteristics of polymer modified and aged bitumens, Doctoral dissertation, University of Nottingham.

Al-Fayyadh, Z.T. and Al-Mosawe, H.M., 2023. The effect of rubber crumbs on marshall properties for warm mix asphalt. Journal of Engineering, 29(6), pp. 46-59. Doi:10.31026/j.eng.2023.06.04

Behzadfar, E., 2014. The flow properties of bitumen in the presence of carbon dioxide (Doctoral dissertation, University of British Columbia). Doi: 10.14288/1.0135569

Błażejowsk, K., and Wójcik-Wiśniewska, M., 2016. Poradnik Asfaltowy, ORLEN asphalt sp, z o.o

Bressi, S., Carter, A., Bueche, N. and Dumont, A.G., 2016. Impact of different ageing levels on binder rheology.

International Journal of Pavement Engineering, 17(5), pp.403-413. Doi:10.1080/10298436.2014.993197

Byrne, D.A., 2005. Recycling of asphalt pavements in new bituminous mixes (Doctoral dissertation). Napier University, School of Built Environment

Campbell, P.G. and Wright, J.R., 1964. Ozonation of asphalt flux. Industrial & Engineering Chemistry Product Research and Development, 3(3), pp.186-194. Doi:10.1021/i360011a005

Chakkoth, U., Krishna, K.R., Ramkumar, M., Rao, P.V.C., Ravindran, P. and Murali Krishnan, J., 2019. Characterization of colloidal stability of blended bitumen. In Transportation Research: Proceedings of CTRG 2017, pp. 883-894. Singapore.

Cheng, Y., Tao, J., Jiao, Y., Guo, Q. and Li, C., 2015. Influence of diatomite and mineral powder on thermal oxidative ageing properties of asphalt. Advances in Materials Science and Engineering, P. 947834. Doi:10.1155/2015/947834

Czajkowski, P., Przyjazny, A. and Boczkaj, G., 2023. Bitumen Aging—Laboratory Simulation Methods Used in Practice and Selected Directions of Research on New Methods. Materials, 16(2), p.853. Doi:10.3390/ma16020853

Das, P.K., Balieu, R., Kringos, N. and Birgisson, B., 2015. On the oxidative ageing mechanism and its effect on asphalt mixtures morphology. Materials and Structures, 48, pp. 3113-3127.

Dickinson, E.J., Nicholas, J.H. and Boas‐Traube, S., 1958. Physical factors affecting the absorption of oxygen by thin films of bituminous road binders. Journal of Applied Chemistry, 8(10), pp.673-687. Doi:10.1002/jctb.5010081010

Edwards, Y. and Isacsson, U., 2005. Wax in bitumen: Part II—characterization and effects. Road materials and pavement design, 6(4), pp.439-468.

Francken, L., Vanelstraete, A. and Verhasselt, A., 1997. Long term ageing of pure and modified bitumen: Influence on the rheological properties and relation with the mechanical performance of asphalt mixtures. In Eighth International Conference on Asphalt Pavements Federal Highway Administration 2, pp. 1259-1278

Gao, Y., Zhang, Y., Omairey, E.L., Al-Malaika, S. and Sheena, H., 2021. Influence of anti-ageing compounds on rheological properties of bitumen. Journal of Cleaner Production, 318, p.128559. Doi:10.1016/j.jclepro.2021.128559.

Gawel, I., Czechowski, F. and Kosno, J., 2016. An environmental friendly anti-ageing additive to bitumen. Construction and Building Materials, 110, pp. 42-47. Doi:10.1016/j.conbuildmat.2016.02.004

Glover, C.J., Davison, R.R., Domke, C.H., Ruan, Y., Juristyarini, P., Knorr, D.B. and Jung, S.H., 2005. Development of a new method for assessing asphalt binder durability with field validation. Texas Dept Transport, 1872, pp.1-334.

Goosen, E.S. and Jenkins, K.J., 2023. Understanding Bitumen Aging through Interrelationships and Aging Ratios. Transportation Research Record, p.1-26. Doi:10.1177/03611981221147519

Greaves, M., Ayatollahi, S., Moshfeghian, M., Alboudwarej, H. and Yarranton, H.W., 2004. Estimation of SARA fraction properties with the SRK EOS. Journal of Canadian Petroleum Technology, 43(09). Doi:10.2118/04-09-02

Großegger, D., 2015. Investigation of aged, non-aged bitumen and their bitumen fractions (Doctoral dissertation). The Vienna University of Technology, Institute of Materials Chemistry.

Guo, X., Sun, M., Dai, W. and Chen, S., 2016. Performance characteristics of silane silica modified asphalt. Advances in Materials Science and Engineering, P. 6731232. Doi:10.1155/2016/6731232

Hagos, E.T., 2008. The effect of aging on binder properties of porous asphalt concrete. Doctoral thesis submitted to Section of Road and Railway Engineering, Faculty of Civil Engineering and Geosciences, Delft University of Technology for the degree of Ph.D. October.

Han, R., 2011. Improvement to a transport model of asphalt binder oxidation in pavements: Pavement temperature modeling, oxygen diffusivity in asphalt binders and mastics, and pavement air void characterization. PhD. Thesis, Texas A&M University.

Handle, F., Harir, M., Füssl, J., Koyun, A.N., Grossegger, D., Hertkorn, N., Eberhardsteiner, L., Hofko, B., Hospodka, M., Blab, R. and Schmitt-Kopplin, P., 2017. Tracking aging of bitumen and its saturate, aromatic, resin, and asphaltene fractions using high-field Fourier transform ion cyclotron resonance mass spectrometry. Energy & Fuels, 31(5), pp.4771-4779. Doi: 10.1021/acs.energyfuels.6b03396

Hrapović, K., 2022. Asphalt and Bitumen Ageing. European Journal of Science, Innovation and Technology, 2(2), pp.49-65.

Hu, Y., Si, W., Kang, X., Xue, Y., Wang, H., Parry, T. and Airey, G.D., 2022. State of the art: Multiscale evaluation of bitumen ageing behaviour. Fuel, 326, p.125045.Doi:10.1016/j.fuel.2022.125045.

Ismael, M., Fattah, M.Y. and Jasim, A.F., 2022. Permanent deformation characterization of stone matrix asphalt reinforced by different types of fibers. Journal of Engineering, 28(2), pp.99-116. Doi:10.31026/j.eng.2022.02.07

Jemere, Y., 2010. Development of a laboratory ageing method for bitumen in porous asphalt. M.Sc. Thesis Civil Engineering from the Road and Railways Engineering Department, Delft University of Technology, Delft, The Netherlands.

Jung, S.H., 2006. The effects of asphalt binder oxidation on hot mix asphalt concrete mixture rheology and fatigue performance. PhD. Thesis, Texas A&M University

Katanalp, B.Y. and Ahmedzade, P., 2023. Rheological Evaluation and Life Cycle Cost Analysis of the Geopolymer Produced from Waste Ferrochrome Electric Arc Furnace Fume as a Composite Component in Bitumen Modification. Journal of Materials in Civil Engineering, 35(11), P.04023401. Doi:10.1061/JMCEE7.MTENG-15906

Król, J.B., Niczke, Ł. and Kowalski, K.J., 2017. Towards understanding the polymerization process in Bitumen bio-

fluxes. Materials, 10(9), p.1058. Doi:10.3390/ma10091058

Lamontagne, J., Dumas, P., Mouillet, V. and Kister, J., 2001. Comparison by Fourier transform infrared (FTIR) spectroscopy of different ageing techniques: application to road bitumens. Fuel, 80(4), pp.483-488. Doi:10.1016/S0016-2361(00)00121-6

Likhterova, N.M., Lunin, V.V., Torkhovskii, V.N., Frantsuzov, V.K. and Kalinicheva, O.N., 1999. Effect of ozonation and strong UV radiation on the rheological properties of atmospheric resid and liquid asphalt. Chemistry and Technology of Fuels and Oils, 35, pp.308-314.

Liu, X., Wu, S., Pang, L., Xiao, Y. and Pan, P., 2014. Fatigue properties of layered double hydroxides modified asphalt and its mixture. Advances in Materials Science and Engineering, P. 868404. Doi:10.1155/2014/868404

Lu, X. and Isacsson, U., 2002. Effect of ageing on bitumen chemistry and rheology. Construction and Building Materials, 16(1), pp.15-22. Doi:10.1016/S0950-0618(01)00033-2

Lucena, M.D.C.C., Soares, S.D.A. and Soares, J.B., 2004. Characterization and thermal behavior of polymer-modified asphalt. Materials Research, 7, pp. 529-534.

Majeed, G.A.W. and Sarsam, S.I., 2021. Assessing the Marshall Properties of Porous Asphalt Concrete. Journal of Engineering, 27(3), pp.113-129. Doi:10.31026/j.eng.2021.03.08

Melkonyan, A. and Wagner, P., 2013. Ozone and its projection in regard to climate change. Atmospheric Environment, 67, pp.287-295. Doi:10.1016/j.atmosenv.2012.10.023

Mills-Beale, J., You, Z., Fini, E., Zada, B., Lee, C.H. and Yap, Y.K., 2014. Aging influence on rheology properties of petroleum-based asphalt modified with biobinder. Journal of Materials in Civil Engineering, 26(2), pp.358-366. Doi:10.1061/(ASCE)MT.1943-5533.000071

Mouillet, V., De la Roche, C., Chailleux, E. and Coussot, P., 2012. Thixotropic behavior of paving-grade bitumens under dynamic shear. Journal of Materials in Civil Engineering, 24(1), pp.23-31. Doi:10.1061/(ASCE)MT.1943-5533.0000354

Mousavi, M., Aldagari, S. and Fini, E.H., 2023. Adsorbing Volatile Organic Compounds within Bitumen Improves Colloidal Stability and Air Quality. ACS Sustainable Chemistry & Engineering. 11(26), pp. 9581–9594. Doi:10.1021/acssuschemeng.3c00539

Mullins, O.C., 2011. The asphaltenes. Annual review of analytical chemistry, 4, pp. 393-418. Doi:10.1146/annurev-anchem-061010-113849

Paliukaite, M., Vaitkus, A. and Zofka, A., 2014. Evaluation of bitumen fractional composition depending on the crude oil type and production technology. In Environmental Engineering. Proceedings of the international conference on environmental engineering. ICEE (Vol. 9, p. 1). pp. 22–23 May, Vilnius, Lithuania.

Petersen, J.C., 2009. A review of the fundamentals of asphalt oxidation: chemical, physicochemical, physical property, and durability relationships. Transportation research circular, (E-C140). http://worldcat.org/issn/00978515

Poulikakos, L.D., Hofko, B., Porot, L., Lu, X., Fischer, H. and Kringos, N., 2016. Impact of temperature on short-and long-term aging of asphalt binders. RILEM Technical Letters, 1, pp.6-9. Doi:10.21809/rilemtechlett.2016.4

Pradhan, S.K., 2023. Short-term and long-term aging effect of the rejuvenation on RAP binder and mixes for sustainable pavement construction. International Journal of Transportation Science and Technology, 12(4), pp.937-954. Doi:10.1016/j.ijtst.2022.09.005

Raab, C., Camargo, I. and Partl, M.N., 2017. Ageing and performance of warm mix asphalt pavements. Journal of Traffic and Transportation Engineering (English Edition), 4(4), pp.388-394. Doi:10.1016/j.jtte.2017.07.002

Rad, F.Y., 2018. Evaluation of the Effect of Oxidative Aging on Asphalt Mixtures for Pavement Performance Prediction. North Carolina State University.

Ramaiah, S., D'Angelo, J. and Dongré, R., 2004. Evaluation of modified German rotating flask. Transportation research record, 1875(1), pp.80-88. Doi:10.3141/1875-09

Read, J. and Whiteoak, D., 2003. The shell bitumen handbook. Thomas Telford.

Remišová, E. and Holý, M., 2018. Impact of bitumen composition on empirical properties. In MATEC Web of Conferences, Vol. 196, P. 04038. Doi:10.1051/matecconf/201819604038

Ryer, A., 1998. Light measurement handbook. Technical Publications Department. International Light, Inc. 17 Graf Road Newburyport. ISBN 0-9658356-9-3

Salehfard, R., Behbahani, H., Dalmazzo, D. and Santagata, E., 2021. Effect of colloidal instability on the rheological and fatigue properties of asphalt binders. Construction and Building Materials, 281, p.122563. Doi:10.1016/j.conbuildmat.2021.122563

Steiner, D., Hofko, B., Hospodka, M., Handle, F., Grothe, H., Füssl, J., Eberhardsteiner, L. and Blab, R., 2016. Towards an optimised lab procedure for long-term oxidative ageing of asphalt mix specimen. International Journal of Pavement Engineering, 17(6), pp.471-477. Doi:10.1080/10298436.2014.993204

Subramanian, M., Deo, M.D. and Hanson, F.V., 1996. Compositional analysis of bitumen and bitumen-derived products. Journal of Chromatographic Science, 34(1), pp.20-26. Doi:10.1093/chromsci/34.1.20

Thyrion, F.C., 2000. Asphalt oxidation. Chapter 16 In Developments in Petroleum Science, 40, pp. 445-474. Doi:10.1016/S0376-7361(09)70287-0

Tia, M. and Wood, L.E., 1983. Use of asphalt emulsion and foamed asphalt in cold-recycled asphalt paving mixtures. Transportation Research Record, 898, pp.315-321.

Valkering, C.P. and Van Gooswilligen, G., 1989. The Role of the Binder Content in the Performance-Related Properties of Asphaltic Mixes for Surface Layers. Proceedings, Journal of the Association of Asphalt Paving Technologists, 58, pp.238-255.

Van den Bergh, W., 2011. The effect of ageing on the fatigue and healing properties of bituminous mortars. Ph.D. thesis submitted to Delft University of Technology. The Netherlands.

Verhasselt, A., 2004. Short-and long-term ageing with RCAT on bituminous mastics. In Proceedings Of The 3rd Eurasphalt And Eurobitume Congress Held Vienna, 2004 (Vol. 2).

Wang, X., Guo, H., Yang, B., Chang, X., Wan, C. and Wang, Z., 2019. Aging characteristics of bitumen from different bituminous pavement structures in service. Materials, 12(3), p.530. Doi:10.3390/ma12030530.

Wu, J., 2009. The influence of mineral aggregates and binder volumetrics on bitumen ageing (Doctoral dissertation, University of Nottingham).

Wu, S., Pang, L., Liu, G. and Zhu, J., 2010. Laboratory study on ultraviolet radiation aging of bitumen. Journal of Materials in Civil Engineering, 22(8), pp.767-772. Doi:10.1061/(ASCE)MT.1943-5533.00000

Xu, M., Zhang, Y. and Zhao, P., 2021. Long-term aging performance study of asphalt with different composition. In IOP Conference Series: Earth and Environmental Science. Vol. 631, No. 1, p. 012050. IOP Publishing. Doi:10.1088/1755-1315/631/1/012050

Yang, C., Xie, J., Wu, S., Amirkhanian, S., Zhou, X., Ye, Q., Yang, D. and Hu, R., 2020. Investigation of physicochemical and rheological properties of SARA components separated from bitumen. Construction and Building Materials, 235, p.117437. Doi:10.1016/j.conbuildmat.2019.117437

Yousif, R.A., Muniandy, R., Hassim, S., Jakarni, F.M. and Aburkaba, E., 2015. An overview of quantification of fatigue resistance of asphalt mixture using pre-aged binder. WALIA journal, 31, pp.125-132.

Yu, X., Wang, Y., Luo, Y. and Yin, L., 2013. The effects of salt on rheological properties of asphalt after long-term aging. The Scientific World Journal, P. 921090. Doi:10.1155/2013/921090

Zhang, H.L., Wang, H.C. and Yu, J.Y., 2011. Effect of aging on morphology of organo‐montmorillonite modified bitumen by atomic force microscopy. Journal of Microscopy, 242(1), pp.37-45. Doi:10.1111/j.1365-2818.2010.03435.x

Zupanick, M. and Baselice, V., 1997. Characterizing asphalt volatility. Transportation research record, 1586(1), pp.1-9. Doi:10.3141/1586-01

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