Selection of Optimal Conditions of Inulin Extraction from Jerusalem Artichoke (Helianthus Tuberosus L.) Tubers by using Ultrasonic Water Bath
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Abstract
Ultrasonic extraction is an inexpensive, simple and efficient alternative to conventional extraction techniques, as compared with other novel extraction techniques such as microwave-assisted extraction & supercritical fluid extraction techniques, the ultrasound apparatus is cheaper and its operation is easier. Ultrasound assisted extraction has risen rapidly in the latest decade, and for most applications it has proven to be effective compared to traditional extraction techniques. In this paper, a method of ultrasonic-assisted extraction was used to extract Inulin from tubers of Jerusalem artichoke, which have been reported to have several medicinal properties and uses. Inulin is a storage carbohydrate found in many plants especially in chicory root, Jerusalem artichoke and dahlia tuber. In this study, the effect of time, temperature, pH and solid to liquid ratio on Inulin extraction from Jerusalem artichoke tubers by using ultrasonic water bath. The highest yield of Inulin were investigated from Jerusalem artichoke tuber was (99.47%) at temperature of 70°C, pH=7, 60 min and ratio of solid to solvent was (10gm/100ml). Then, The UV detector by colorimetric method with vanillin–sulfuric acid was used for the quantification of Inulin.
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Abdul razak, M. S., 2009, Ultrasonic Extraction of Antioxidant Compound from Red Pitaya, A thesis submitted to Faculty of Chemical and Natural Resources Engineering. Universiti Malaysia Pahang.
Abou-Arab, A. A., Talaat, H.A.and Abu-Salem, F. M., 2011, Physico-chemical Properties of Inulin Produced from Jerusalem Artichoke Tubers on Bench and Pilot Plant Scale, Australian Journal of Basic and Applied Sciences, Vol.5 , No. 5, PP. 1297-1309.
Chen, L., Jin, H., Wang, L., Sun, L., Xu, H., Ding, L., Yu, A. and Zhang, H., 2008 , Dynamic Ultrasound-Assisted Extraction Coupled On-Line With Solid Support Derivatization And High-Performance Liquid Chromatography For The Determination of Formaldehyde In Textiles, Journal of Chromatography A, Vol.1192, PP. 89–94.
Costa , S. B., Duarte, C., Bourbon, A. I., Pinheiro, A. C., Januário, M. I. N., Vicente, A. A., Costa, M. L. and Delgadillo, I., 2013, Inulin Potential for Encapsulation and Controlled Delivery of Oregano Essential Oil, Food Hydrocolloids, Vol. 33,PP. 199-206.
Dobre, T., Stroescu, M., Stoica, A., Draghici, E. and Antohe, N. 2008, Inulin Extraction and Encapsulation, Chem. Bull. "POLITEHNICA" Univ., Vol. 53, No. 67, PP. 1-2.
Dobre,T., Parvulescu, O. C., Stoica, A. and Stroescu, M., 2010, Experimental Investigation and Modeling of Inulin and Glycyrrhizin Extraction, REV. CHIM. Vol. 61 No. 1, PP. 82-86.
Firdaus, M. T., Izam, A., Prasad, R. and Rosli, 2010, Ultrasonic-Assisted Extraction of Triterpenoid Saponins from Mangrove Leaves, the 13th Asia Pacific Confederation of Chemical Engineering Congress, October, 5-8, Taipei.
Gaafar ,A. M., Serag El-Din, M. F., Boudy E. A. and El-Gazar ,H. H., 2010, Extraction Conditions of inulin from Jerusalem Artichoke Tubers and its Effects on Blood Glucose and Lipid Profile in Diabetic Rats, Journal of American Science,vol.6, No.5, PP. 36-43.
Glibowski, P. and Bukowska, A., 2011, The Effect of pH, Temperature and Heating Time on Inulin Chemical Stability, Acta Sci. Pol., Technol, Aliment,Vol. 10, No.2, PP. 189-196.
Ince, A. E., Şahin, S. and Şümnü, S. G., 2013, Extraction of phenolic compounds from Melissa using Microwave and Ultrasound, Turkish Journal of Agriculture and Forestry,Vol.37, PP. 69-75.
Jalbani, N., Kazi, T. G., Arain, B. M., Jamali, M.K., Afridi, H. I. and Sarfraz, R.A., 2006, Application of Factorial Design in Optimization of Ultrasonic-Assisted Extraction of Aluminum in Juices and Soft Drinks, Talanta, Vol. 70, PP. 307–314.
Leite, J. T. C., Martinelli, P., Murr, F. E. X. and Park, K. J., 2004, Study of the Inulin Concentration by Physical Methods, Proceedings of the 14th International Drying Symposium (IDS 2004), Brazil, Vol. B, PP. 868-875.
Li, H., Pordesimo, L. and Weiss, J., 2004, High Intensity Ultrasound-Assisted Extraction of Oil from Soybeans, Food Research International, Vol. 37, PP. 731–738.
Li, Z. and Zhou, L., 2008, Rapid And Low Cost Determination of Cadmium in Whole Blood by Hydride Generation Atomic Fluorescence Spectrometry after Ultrasound-Assisted Sample Preparation, J. Braz. Chem. Soc., Vol. 19, No. 7, PP. 1347-1354.
Nogueira, R. I., Park, K. J., Deyrmendjian, E., Bruns, R. E. and Bortoloti, J. A., 2007, Apparent Viscosity of Formulations of Inulin Chicory Extract (Cichorium Intybus L ) with Modified and Hydrolyzed Starches, Revista Brasileira de Produtos Agroindustriais, Campina Grande, Vol. 9, No.1, PP. 7-15.
Panchev, I., Delchev, N., Kovacheva, D. and Slavov, A., 2011, Physicochemical Characteristics of Inulins Obtained from Jerusalem Artichoke (Helianthus tuberosus L.), Eur. Food Res Technol, Vol. 233, PP. 889–896.
Plaza, M., Avalo, B., Cifuentes, A. and Ibáñez, E., 2008, Pressurized Liquid Extraction and Ultrasound-Assisted Extraction of Functional Ingredients from Chlorella Vulgaris.Chemical Characterization Using HPLC-DAD And GC-MS.
Ripoll, C., Flourie, B., Megnien, S., Hermand, O., and Janssens, M., 2010, Gastrointestinal Tolerance to an Inulin-rich Soluble Roasted Chicory Extract after Consumption in Healthy Subjects, Nutrition,Vol. 26, PP. 799–803.
Saengkanuk, A., Nuchadomrong, S., Jogloy, S. , Patanothai, A. and Srijaranai, S. , 2011, A simplified Spectrophotometric Method for the Determination of Inulin in Jerusalem Artichoke (Helianthus tuberosus L.) tubers, Eur Food Res Technol, Vol. 233, PP.609–616.
Toneli, J. T. C. L., Park, K. J., Ramalho, J. R. P., Murr, F. E. X. and Fabbro, I. M. D., 2008, Rheological Characterization of Chicory Root (Cichorium Intybus L.) Inulin Solution, Brazilian Journal of Chemical Engineering, Vol. 25, No. 03, PP. 461 – 471.
Winarti, S., Harmayani, E. and Nurismanto, R., 2011, Extraction of Inulin from Various Yam Tubers (Dioscorea spp.), the 12th Asean Food Conference, PP. 669-773.
Yang, B., Jiang, Y., Zhao, M., Shi, J. and Wang, L. 2008, Effects of Ultrasonic Extraction on the Physical and Chemical Properties of Polysaccharides from Longan Fruit Pericarp, Polymer Degradation and Stability, Vol. 93, PP. 268-272.